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4-(2,4,6-trinitroanilino)benzoic acid

Smith, Graham, Wermuth, Urs D., & White, Jonathan M. (2007) 4-(2,4,6-trinitroanilino)benzoic acid. Acta Crystallographica. Section E: Structure Reports Online, E63(12), o4803-sup8.

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Abstract

4-(2,4,6-trinitroanilino)benzoic acid (p-picraminobenzoic acid), C13H8N3O8, obtained by the reaction of 2,4,6-trinitrobenzenesulfonic acid (picrylsulfonic acid) with 4-aminobenzoic acid in 2-propanol-water, forms a two-dimensional hydrogen-bonded network based on centrosymmetric cyclic R2/2(8) carboxylic acid dimers which are extended through lateral N-H...O(carboxyl) interactions. The amino group also makes an intramoleclar N-H...O(nitro) hydrogen bond, while the two aromatic ring systems are, as expected, non-coplanar, the C-C-N-C torsion angles being 152.0(2)(picryl) and 136.1(2)deg. (benzoic acid).

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3 citations in Scopus
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3 citations in Web of Science®

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154 since deposited on 26 Nov 2007
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ID Code: 10915
Item Type: Journal Article
Keywords: 4, (2, 4, 6, trinitroanilino)benzoic acid, crystal structure
DOI: 10.1107/S1600536807058497
ISSN: 1600-5368
Subjects: Australian and New Zealand Standard Research Classification > CHEMICAL SCIENCE (030000) > PHYSICAL CHEMISTRY (INCL. STRUCTURAL) (030600) > Structural Chemistry and Spectroscopy (030606)
Divisions: Past > QUT Faculties & Divisions > Faculty of Science and Technology
Copyright Owner: Copyright 2007 International Union of Crystallography
Copyright Statement: Reproduced in accordance with the copyright policy of the publisher.
Deposited On: 26 Nov 2007
Last Modified: 29 Feb 2012 23:39

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