Synthesis and surface characterization of yttrium doped boehmite nanofibers
Yttrium doped boehmite nanofibres with varying yttrium content have been synthessied at low temperatures using a soft-chemistry route in the presence of polyglycol ether surfactant. The effect of yttrium content, hydrothermal temperature on the growth of boehmite nanostructures was systematically studied. Nanofibres were formed in all samples with varying doped Y% treated at 100 degrees Celsius; large Y(OH)3 crystals were also formed at high yttrium doping. Treated at an elevated temperatures resulted in a remarkable changes in size and morphology for samples with the same doped Y content. The resultant nanofibres were characterized by X-ray diffraction (XRD), transmission electron microscopy (TEM), selected area electron diffraction (SAED), energy-dispersive X-ray analysis (EDX), N2 adsorption and thermogravimetric analysis. The detailed characterization and discussion on the Y doped nanostructures is presented.
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|Item Type:||Journal Article|
|Keywords:||boehmite, surface characterisation, nanofibre, surface area, transmission electron microscopy|
|Subjects:||Australian and New Zealand Standard Research Classification > CHEMICAL SCIENCE (030000) > PHYSICAL CHEMISTRY (INCL. STRUCTURAL) (030600) > Structural Chemistry and Spectroscopy (030606)|
Australian and New Zealand Standard Research Classification > CHEMICAL SCIENCE (030000) > PHYSICAL CHEMISTRY (INCL. STRUCTURAL) (030600)
Australian and New Zealand Standard Research Classification > CHEMICAL SCIENCE (030000) > PHYSICAL CHEMISTRY (INCL. STRUCTURAL) (030600) > Colloid and Surface Chemistry (030603)
|Divisions:||Past > QUT Faculties & Divisions > Faculty of Science and Technology|
|Copyright Owner:||Copyright 2008 Elsevier|
|Copyright Statement:||Reproduced in accordance with the copyright policy of the publisher.|
|Deposited On:||28 Aug 2008|
|Last Modified:||29 Feb 2012 23:46|
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