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4-Chloroanilinium 2-carboxy-4,5-dichlorobenzoate

Smith, Graham, Wermuth, Urs D., & White, Jonathan M. (2009) 4-Chloroanilinium 2-carboxy-4,5-dichlorobenzoate. Acta Crystallographica Section E, 65, o2111.

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Abstract

The structure of the 1:1 proton-transfer compound of 4-chloroaniline with 4,5-dichlorophthalic acid (DCPA), viz. C6H7ClN+ C8H3Cl2O4-, has been determined at 130 K. The non-planar hydrogen phthalate anions and the 4-chloroanilinium cations form two-dimensional O-H...O and N-H...O hydrogen-bonded substructures which have no peripheral extension. Between the sheets there are weak \p--\p associations between alternating cation--anion aromatic ring systems [shortest centroid separation, 3.735(4)A].

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6 citations in Web of Science®

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22 since deposited on 11 Oct 2009
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ID Code: 27839
Item Type: Journal Article
Keywords: crystal structure, hydrogen bonding, proton-transfer, 4,5-dichlorophthalic acid
DOI: 10.1107/S160053680903044X
ISSN: 1600-5368
Subjects: Australian and New Zealand Standard Research Classification > CHEMICAL SCIENCE (030000) > PHYSICAL CHEMISTRY (INCL. STRUCTURAL) (030600) > Structural Chemistry and Spectroscopy (030606)
Divisions: Past > QUT Faculties & Divisions > Faculty of Science and Technology
Past > Schools > School of Physical & Chemical Sciences
Copyright Owner: Copyright 2009 Blackwell Publishing and the authors.
Copyright Statement: The definitive version is available at www.blackwell-synergy.com
Deposited On: 12 Oct 2009 09:28
Last Modified: 01 Mar 2012 00:09

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