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Two pseudopolymorphic hydrates of brucine: brucine-water (1/4) and brucine-water (1/5.25) at 130 K

Smith, Graham, Wermuth, Urs D., Healy, Peter C., & White, Jonathan M. (2006) Two pseudopolymorphic hydrates of brucine: brucine-water (1/4) and brucine-water (1/5.25) at 130 K. Acta Crystallographica. Section C: Crystal Structure Communications, 62(1), o203-o207.

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Abstract

The structures of two pseudopolymorphic hydrates of brucine, C23H26N2O4·4H2O, (I), and C23H26N2O4·5.25H2O, (II), have been determined at 130 K. In both (I) and (II) (which has two independent brucine molecules together with 10.5 water molecules of solvation in the asymmetric unit), the brucine molecules form head-to-tail sheet substructures, which associate with the water molecules in the interstitial cavities through hydrogen-bonding associations and, together with water-water associations, give three-dimensional framework structures.

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164 since deposited on 15 Jan 2007
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ID Code: 4900
Item Type: Journal Article
Additional Information: Author contact details: g.smith@qut.edu.au
DOI: 10.1107/S0108270106005944
ISSN: 0108-2701
Subjects: Australian and New Zealand Standard Research Classification > CHEMICAL SCIENCE (030000)
Divisions: Past > QUT Faculties & Divisions > Faculty of Science and Technology
Copyright Owner: Copyright 2006 International Union of Crystallography
Copyright Statement: The definitive version is available at www.blackwell-synergy.com
Deposited On: 15 Jan 2007
Last Modified: 29 Feb 2012 23:26

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