2,3-Dimethoxy-10-oxostrychnidinium 3-carboxybenzoate trihydrate: the 1:1 proton-transfer compound of brucine with isophthalic acid
Smith, Graham, Wermuth, Urs D., Young, David J., & White, Jonathan M. (2006) 2,3-Dimethoxy-10-oxostrychnidinium 3-carboxybenzoate trihydrate: the 1:1 proton-transfer compound of brucine with isophthalic acid. Acta Crystallographica. Section E: Structure Reports Online, 62(4), o1553-o1555.
The structure of the title compound C23H27N2O4+ . C8 H5O4 . 3H2O, has been determined at 130 K. The hydrogenisophthalate anions and the water molecules (one of which is disordered over two approximately equal sites) associate through extensive hydrogen-bonding interactions, including those with the common undulating brucinium cation layer substructures, forming a three-dimensional framework structure.
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|Item Type:||Journal Article|
|Keywords:||single crystal structure, brucine, proton, transfer compounds|
|Subjects:||Australian and New Zealand Standard Research Classification > CHEMICAL SCIENCE (030000) > PHYSICAL CHEMISTRY (INCL. STRUCTURAL) (030600) > Structural Chemistry and Spectroscopy (030606)|
|Divisions:||Past > QUT Faculties & Divisions > Faculty of Science and Technology|
|Copyright Owner:||Copyright 2006 International Union of Crystallography|
|Copyright Statement:||The definitive version is available at www.blackwell-synergy.com|
|Deposited On:||07 Feb 2007|
|Last Modified:||29 Feb 2012 23:18|
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