Direct iodination of isoindolines and isoindoline nitroxides as precursors to functionalized nitroxides
Fairfull-Smith, Kathryn E., Debele, Emmanuel, Allen, Jesse, Prfunder, Michael, & McMurtrie, John (2013) Direct iodination of isoindolines and isoindoline nitroxides as precursors to functionalized nitroxides. European Journal of Organic Chemistry, 2013(22), pp. 4829-4835.
A new method for the direct aryl iodination of isoindolines and isoindoline nitroxides which utilizes periodic acid and potassium iodide in sulfuric acid is presented. Di-iodo functionalized tetramethyl and tetraethyl isoindolines and a di-iodo tetramethyl isoindoline nitroxide were prepared in high yield (70-82%). The analogous mono-iodo species were afforded in modest yield (34-48%). Iodinated nitrones were also obtained from a tetraethyl isoindoline nitroxide.
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|Item Type:||Journal Article|
|Keywords:||Synthetic methods, Aromatic substitution, Halogenation, radicals, Nitrogen oxides|
|Subjects:||Australian and New Zealand Standard Research Classification > CHEMICAL SCIENCE (030000)|
|Divisions:||Current > Schools > School of Chemistry, Physics & Mechanical Engineering
Past > QUT Faculties & Divisions > Faculty of Science and Technology
Current > QUT Faculties and Divisions > Science & Engineering Faculty
|Copyright Owner:||Copyright 2013 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim|
|Deposited On:||28 Jan 2014 04:23|
|Last Modified:||30 Jan 2014 05:22|
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