A novel protecting group methodology for syntheses using nitroxides
Chalmers, Benjamin, Morris, Jason, Fairfull-Smith, Kathryn, Grainger, Richard, & Bottle, Steven (2013) A novel protecting group methodology for syntheses using nitroxides. Chemical Communications, 2013(88), pp. 10382-10384.
The methoxyamine group represents an ideal protecting group for the nitroxide moiety. It can be easily and selectively introduced in high yield (typically >90%) to a range of functionalised nitroxides using FeSO4.7H2O and H2O2 in DMSO. Its removal is readily achieved under mild conditions in high yield (70-90%) using mCPBA in a Cope-type elimination process.
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|Item Type:||Journal Article|
|Subjects:||Australian and New Zealand Standard Research Classification > CHEMICAL SCIENCE (030000) > ORGANIC CHEMISTRY (030500) > Free Radical Chemistry (030501)|
|Divisions:||Current > Schools > School of Chemistry, Physics & Mechanical Engineering
Current > QUT Faculties and Divisions > Science & Engineering Faculty
|Copyright Owner:||Copyright 2013 Royal Society of Chemistry|
|Deposited On:||29 Jan 2014 00:34|
|Last Modified:||30 Jan 2014 04:55|
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