Rediscovering the double Friedel-Crafts acylation : an expedient entry to phenanthrene-9,10-diones
Crosta, Nicoletta, Müller, Sebastian, Gradl, Dietmar, Masters, Kye-Simeon, & Bräse, Stefan (2013) Rediscovering the double Friedel-Crafts acylation : an expedient entry to phenanthrene-9,10-diones. Synlett, 24(8), pp. 951-954.
The double Friedel–Crafts acylation of readily accessible biaryls with oxalyl chloride delivers the respective phenanthrene-9,10-diones, providing an alternative to the traditional methods, which require harsh oxidizing conditions and multistep sequences. This simple method allows the synthesis of various symmetrical and non-symmetrical targets, and is even effective for the synthesis of the parent ring system from (unactivated) biphenyl.
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|Item Type:||Journal Article|
|Subjects:||Australian and New Zealand Standard Research Classification > CHEMICAL SCIENCE (030000) > ORGANIC CHEMISTRY (030500) > Organic Chemical Synthesis (030503)|
|Divisions:||Current > Schools > School of Chemistry, Physics & Mechanical Engineering
Current > QUT Faculties and Divisions > Science & Engineering Faculty
|Copyright Owner:||Copyright 2013 Georg Thieme Verlag|
|Deposited On:||02 Apr 2014 23:19|
|Last Modified:||03 Apr 2014 22:20|
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