Rediscovering the double Friedel-Crafts acylation : an expedient entry to phenanthrene-9,10-diones

Crosta, Nicoletta, Müller, Sebastian, Gradl, Dietmar, Masters, Kye-Simeon, & Bräse, Stefan (2013) Rediscovering the double Friedel-Crafts acylation : an expedient entry to phenanthrene-9,10-diones. Synlett, 24(8), pp. 951-954.

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Abstract

The double Friedel–Crafts acylation of readily accessible biaryls with oxalyl chloride delivers the respective phenanthrene-9,10-diones, providing an alternative to the traditional methods, which require harsh oxidizing conditions and multistep sequences. This simple method allows the synthesis of various symmetrical and non-symmetrical targets, and is even effective for the synthesis of the parent ring system from (unactivated) biphenyl.

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2 citations in Scopus
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1 citations in Web of Science®

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ID Code: 69690
Item Type: Journal Article
Refereed: Yes
DOI: 10.1055/s-0032-1318481
ISSN: 1437-2096
Subjects: Australian and New Zealand Standard Research Classification > CHEMICAL SCIENCE (030000) > ORGANIC CHEMISTRY (030500) > Organic Chemical Synthesis (030503)
Divisions: Current > Schools > School of Chemistry, Physics & Mechanical Engineering
Current > QUT Faculties and Divisions > Science & Engineering Faculty
Copyright Owner: Copyright 2013 Georg Thieme Verlag
Deposited On: 02 Apr 2014 23:19
Last Modified: 03 Apr 2014 22:20

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