In situ reaction furnace for real-time XRD studies
Riello, Pietro, Lausi, Andrea, MacLeod, Jennifer, Plaisier, Jasper Rikkert, Zerauschek, Giulio, & Fornasiero, Paolo (2013) In situ reaction furnace for real-time XRD studies. Journal of Synchrotron Radiation, 20(1), pp. 194-196.
The new furnace at the Materials Characterization by X-ray Diffraction beamline at Elettra has been designed for powder diffraction measurements at high temperature (up to 1373 K at the present state). Around the measurement region the geometry of the radiative heating element assures a negligible temperature gradient along the capillary and can accommodate either powder samples in capillary or small flat samples. A double capillary holder allows flow-through of gas in the inner sample capillary while the outer one serves as the reaction chamber. The furnace is coupled to a translating curved imaging-plate detector, allowing the collection of diffraction patterns up to 2[theta] [asymptotically equal to] 130°.
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|Item Type:||Journal Article|
|Keywords:||X-ray diffraction; in situ; temperature control; catalytic characterization|
|Divisions:||Current > Schools > School of Chemistry, Physics & Mechanical Engineering
Current > QUT Faculties and Divisions > Science & Engineering Faculty
|Copyright Owner:||Copyright 2013 International Union of Crystallography|
|Deposited On:||06 Apr 2016 06:10|
|Last Modified:||15 Apr 2016 03:17|
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