In situ reaction furnace for real-time XRD studies

Riello, Pietro, Lausi, Andrea, MacLeod, Jennifer, Plaisier, Jasper Rikkert, Zerauschek, Giulio, & Fornasiero, Paolo (2013) In situ reaction furnace for real-time XRD studies. Journal of Synchrotron Radiation, 20(1), pp. 194-196.

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The new furnace at the Materials Characterization by X-ray Diffraction beamline at Elettra has been designed for powder diffraction measurements at high temperature (up to 1373 K at the present state). Around the measurement region the geometry of the radiative heating element assures a negligible temperature gradient along the capillary and can accommodate either powder samples in capillary or small flat samples. A double capillary holder allows flow-through of gas in the inner sample capillary while the outer one serves as the reaction chamber. The furnace is coupled to a translating curved imaging-plate detector, allowing the collection of diffraction patterns up to 2[theta] [asymptotically equal to] 130°.

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ID Code: 89962
Item Type: Journal Article
Refereed: Yes
Additional URLs:
Keywords: X-ray diffraction; in situ; temperature control; catalytic characterization
DOI: 10.1107/S0909049512039246
ISSN: 1600-5775
Divisions: Current > Schools > School of Chemistry, Physics & Mechanical Engineering
Current > QUT Faculties and Divisions > Science & Engineering Faculty
Copyright Owner: Copyright 2013 International Union of Crystallography
Deposited On: 06 Apr 2016 06:10
Last Modified: 15 Apr 2016 03:17

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