Combined SEM/EDX and micro-Raman spectroscopy analysis of uranium minerals from a former uranium mine

Stefaniak, Elzbieta, alsecz, Anita, , Mathe, Zoltan, Sajo, Istvan, Torok, Szabina, Worobiec, Anna, & Van Grieken, Rene (2009) Combined SEM/EDX and micro-Raman spectroscopy analysis of uranium minerals from a former uranium mine. Journal of Hazardous Materials, 168(1), pp. 416-423.

[img]
Preview
Accepted Version (PDF 563kB)
c20971.pdf.

View at publisher

Description

Samples of the secondary uranium minerals collected in the abandoned uranium mine at Pecs (Hungary) were investigated by two micro-techniques: scanning electron microscopy (SEM/EDX) and micro-Raman spectroscopy (MRS). They were applied to locate U-rich particles and identify the chemical form and oxidation state of the uranium compounds. The most abundant mineral was a K and/or Na uranyl sulphate (zippeite group). U(VI) was also present in the form of a trioxide; evidently in much lower content.than sulphate. Few particles with U3O8 and uraninite (primary mineral exploited formerly in this mine) were also detected. This research has shown the successful application of micro-Raman spectroscopy for the identification of uranyl mineral species on the level of individual particles.

Impact and interest:

45 citations in Scopus
39 citations in Web of Science®
Search Google Scholar™

Citation counts are sourced monthly from Scopus and Web of Science® citation databases.

These databases contain citations from different subsets of available publications and different time periods and thus the citation count from each is usually different. Some works are not in either database and no count is displayed. Scopus includes citations from articles published in 1996 onwards, and Web of Science® generally from 1980 onwards.

Citations counts from the Google Scholar™ indexing service can be viewed at the linked Google Scholar™ search.

Full-text downloads:

821 since deposited on 03 Jun 2009
26 in the past twelve months

Full-text downloads displays the total number of times this work’s files (e.g., a PDF) have been downloaded from QUT ePrints as well as the number of downloads in the previous 365 days. The count includes downloads for all files if a work has more than one.

ID Code: 20971
Item Type: Contribution to Journal (Journal Article)
Refereed: Yes
Measurements or Duration: 8 pages
Keywords: Micro-Raman Spectroscopy, SEM/EDX, Uranium Mine, Uranium Minerals, Uranyl Ion
DOI: 10.1016/j.jhazmat.2009.02.057
ISSN: 0304-3894
Pure ID: 31935626
Divisions: Past > QUT Faculties & Divisions > Faculty of Science and Technology
Past > QUT Faculties & Divisions > Science & Engineering Faculty
Current > Research Centres > Australian Research Centre for Aerospace Automation
Copyright Owner: Consult author(s) regarding copyright matters
Copyright Statement: This work is covered by copyright. Unless the document is being made available under a Creative Commons Licence, you must assume that re-use is limited to personal use and that permission from the copyright owner must be obtained for all other uses. If the document is available under a Creative Commons License (or other specified license) then refer to the Licence for details of permitted re-use. It is a condition of access that users recognise and abide by the legal requirements associated with these rights. If you believe that this work infringes copyright please provide details by email to qut.copyright@qut.edu.au
Deposited On: 03 Jun 2009 23:26
Last Modified: 27 May 2024 20:52